142 20, Praha 4
phone: +420-241 062 487, +420-241 062 499
fax: +420-241 062 499
e-mail: stanomusil@biomed.cas.cz
Born:
4.2. 1983 in Prague, Czech Republic
Education:
2011 Ph.D., RNDr. (Rerum Naturalium Doctor)
Department of Analytical Chemistry, Faculty of Science, Charles University in Prague and Institute of Analytical Chemistry of the ASCR, v.v.i., 2007–2011, supervisor T. Matoušek
Ph.D. Thesis: Contributions to volatile compound generation of arsenic, silver and gold by tetrahydroborate reaction for atomic absorption spectrometry
2007 MSc. (Mgr.)
graduated (Analytical Chemistry), Faculty of Science, Charles University, Prague, master thesis elaborated at Institute of Analytical Chemistry of the ASCR, v.v.i., Prague, 2005–2007, supervisor T. Matoušek
Master thesis: On-line pre-reduction of pentavalent arsenicals by thioglycolic acid for speciation analysis by selective hydride generation-cryotrapping-AAS
2002-2007
undergraduate student (Analytical Chemistry), Faculty of Science, Charles University in Prague
1998-2002
Gymnasium Budějovická (high school), Prague
Language skills
English (advanced, FCE – First Certificate in English in 2008)
Other activities
2011 Authorization of special professional competence to perform the activities especially important from the viewpoint of radiation protection to the extent covering: a) continuous supervision over compliance with requirements for radiation protection as a supervising person and b) a person with direct responsibility for radiation protection at workplaces with open emitters of II. category, pursuant to § 9 of Decree No. 146/1997 Coll., as amended by Decree No. 315/2002 Coll.
Current research interests
Speciation analysis of arsenic – selective generation of methylsubstituted arsines with cryogenic collection and detection by AAS or AFS, development of the apparatus design, optimization of experimental parameters, analysis of real samples (water, cell and tissue samples).
Volatile species generation of transition metals – development of the apparatus design and optimization of experimental parameters, searching for the nature of volatile species, radiotracer study of generation efficiency.
In-situ collection – preconcentration of volatile species of Ag in new quartz/ceramic/metallic tube atomizer designs, development of the ideal apparatus design and optimization of experimental parameters.
Radiotracer techniques – application of radioactive indicators for investigation of newly developed methods, spatial distribution of analyte in the apparatus by image plate autoradiography and estimation of efficiency in individual steps of volatile species generation.
Participation in grant projects
Member of the research team
Development of methods of arsenic speciation analysis for application in toxicological research, Ministry of education and sports of the Czech Republic, Kontakt II-LH12040, 2012–2014.
Speciation analysis of toxicologically important As species: development of instrumentation and methodologies, GA CR 203/09/1783, 2009–2011.
Development of instrumentation and methodologies for analysis of As species, Gillings Innovation Labs project, 2008–2010.
Improvement of Cryogenic Trapping Arrangement for Arsenic Speciation by Hydride Generation – Atomic Absorption Spectrometry, GA UK, Grant No. 133008, 2008–2010.
Application of chemical generation of volatile forms of transition and noble metals to the methods of analytical atomic spectrometry, GA ASCR, Grant No. IAA400310704, 2007–2009.
Speciation analysis by hydride generation atomic fluorescence and atomic absorption spectrometry, GA AS CR, Grant No. A400310507, 2005–2009.
Optimized Hydride Generation Systems for Arsenic Speciation Analysis, NIH/FIRCA, project no. 1 R03 TW007057-01, 2004–2007
International visits
FEBRUARY 2013 – MAY 2013 (3 MONTHS)
Postdoc fellowship in Trace Element Speciation Laboratory (TESLA), College of Physical Sciences, University of Aberdeen, Aberdeen, Scotland, UK (prof. Jörg Feldmann), supported by Internal support of projects for international collaboration of the AS CR (Reg. no. M200311271) and by Journal Grant for International Authors from Royal Society of Chemistry.
Honors and awards
2011
1st Poster Prize at the 3rd International Symposium on Metallomics, Münster, Germany, 15.–18.6.2011
2010
1st Poster Prize at the XIV. Czech-Slovak spectroscopic conference sponsored by Thermo Fisher Scientific, Litomyšl, 31.5.–3.6.2010.
2009
JAAS Poster Prize at the Colloquium Spectroscopicum Internationale XXXVI, Budapest, Hungary, 30.8.–3.9.2009.
Analyst Poster Prize at the Colloquium Spectroscopicum Internationale XXXVI, Budapest, Hungary, 30.8.–3.9.2009.
2007
Spectroscopic Society of Ioannes Marcus Marci, Prague: The best Master thesis in the field of spectroscopy competition – 2.prize
List of papers:
MATOUŠEK T., CURRIER J. M., TROJÁNKOVÁ N., SAUNDERS R. J., ISHIDA M. C., GONZÁLEZ-HORTA C., MUSIL S., MESTER Z., STÝBLO M., DĚDINA J.: Selective hydride generation – cryotrapping – ICP-MS for arsenic speciation analysis at picogram levels: analysis of river and sea water reference materials and human bladder epithelial cells. Journal of Analytical Atomic Spectrometry, accepted.
MUSIL S., DĚDINA J.: A sapphire tube atomizer for on-line atomization and in situ collection of bismuthine for atomic absorption spectrometry.
Journal of Analytical Atomic Spectrometry, 28 (2013), 593-600.
KRATZER J., MUSIL S., VOBECKÝ M., DĚDINA J.: Hydride generation – in-atomizer collection of Pb in quartz tube atomizers for atomic absorption spectrometry – a 212Pb radiotracer study.
Journal of Analytical Atomic Spectrometry, 28 (2013), 344-353.
MUSIL S., KRATZER J., VOBECKÝ M., MATOUŠEK, T.: In situ collection of volatile silver species in a new modular quartz tube atomizer for atomic absorption spectrometry.
Journal of Analytical Atomic Spectrometry, 27 (2012), 1382-1390.
ARSLAN Y., MATOUŠEK T., KRATZER J., MUSIL S., BENADA O., VOBECKÝ M., ATAMAN O. Y., DĚDINA J.:
Gold volatile compound generation: optimization, efficiency and characterization of the generated form.
Journal of Analytical Atomic Spectrometry, 26 (2011), 828-837.
TAURKOVÁ P., SVOBODA M., MUSIL S., MATOUŠEK, T.:
Loss of di- and trimethylarsine on Nafion membrane dryers following hydride generation.
Journal of Analytical Atomic Spectrometry, 26 (2011), 220-223
MUSIL S., KRATZER J., VOBECKÝ M., BENADA O., MATOUŠEK, T.:
Silver chemical vapor generation for atomic absorption spectrometry: minimization of transport losses, interferences and application to water analysis.
Journal of Analytical Atomic Spectrometry, 25 (2010), 1618-1626.
MUSIL S., KRATZER J., VOBECKÝ M., HOVORKA J., BENADA O., MATOUŠEK T.:
Chemical vapor generation of silver for atomic absorption spectrometry with the multiatomizer: radiotracer efficiency study and characterization of silver species.
Spectrochimica Acta Part B: Atomic Spectroscopy, 64 (2009), 1240-1247.
MUSIL S., MATOUŠEK T.:
On-line pre-reduction of pentavalent arsenicals by thioglycolic acid for speciation analysis by selective hydride generation-cryotrapping-atomic absorption spectrometry.
Spectrochimica Acta Part B: Atomic Spectroscopy, 63 (2008), 685-691.
Patents and patent applications
DĚDINA J., MUSIL S., D´ULIVO A.: Dvoukanálová stínicí jednotka atomizátoru pro atomovou fluorescenční spektrometrii, PV 2012-398, Industrial Property Office, submitted 14.6.2012.
MUSIL S., MATOUŠEK T.: Modulární atomizátor pro in-situ prekoncentraci a detekci těkavých specií kovů, Czech patent no. 353735, issued by Industrial Property Office of the Czech Republic (27.2. 2013).
List of conference contributions:
MUSIL S., MATOUŠEK T., RYCHLOVSKÝ P.: On-line pre-reduction of pentavalent arsenicals by thioglycolic acid for speciation analysis by selective hydride generation-cryotrapping-AAS. In: XIII. Spectroscopic conference. Lednice, 18.-21. June 2007, p. 77.
MUSIL S., MATOUŠEK T., RYCHLOVSKÝ P.: On-line Pre-reduction of Pentavalent Arsenicals by Thioglycolic Acid for Speciation Analysis by Selective Hydride Generation-Cryotrapping-AAS. In: Colloquium Spectroscopicum Internationale XXXV. Xiamen, China, 21.-27. September 2007, p. 403.
MUSIL S., KRATZER J., VOBECKÝ M., RYCHLOVSKÝ P., MATOUŠEK T.: Chemical vapour generation of silver as a method for sample introduction for atomic absorption spectrometry. In: 4th International Student Conference: “Modern Analytical Chemistry”, Book of proceedings, Prague, 28.-29. January 2008, ISBN 978-80-903103-2-2, p. 113.-117.
MUSIL S., MATOUŠEK T., RYCHLOVSKÝ P.: Thioglycolic acid as on-line pre-reductant for speciation analysis of arsenic by selective hydride generation-cryotrapping-AAS. In: 4th International Student Conference: “Modern Analytical Chemistry”, Book of proceedings, Prague, 28.-29. January 2008, ISBN 978-80-903103-2-2, p. 123.-129.
MUSIL S., KRATZER J., VOBECKÝ M., MATOUŠEK T.: Chemical vapour generation of silver for AAS: assessement of introduction efficiency by 111 Ag radiotracer experiments. In: Tenth Rio Symposium on Atomic Spectrometry. Salvador – Bahia, Brazil, 7.-12. September 2008, p. 142.
MATOUŠEK T., MUSIL S., HOVORKA J.: Chemical vapour generation of silver for AAS: tracking silver nanoparticles in the gaseous phase. In: Tenth Rio Symposium on Atomic Spectrometry. Salvador – Bahia, Brazil, 7.-12. September 2008, p. 143.
MUSIL S., MATOUŠEK T., RYCHLOVSKÝ P.: On-line pre-reduction of pentavalent arsenicals by thioglycolic acid for speciation analysis by HG-CT-AAS. In: Workshop of Speciation Analysis, Nová Olešná, Czech Republic, Book of Abstracts, 22.-25. June 2009, p. 18.-19.
ARSLAN, Y., MATOUŠEK, T., KRATZER, J., MUSIL S., ATAMAN, O.Y., DĚDINA J.: Determination of Gold by Chemical Hydride Generation Atomic Absorption Spectrometry. In: CSI XXXVI – Colloquium Spectroscopicum Internationale, Book of Abstracts, Budapest, Hungary, 30. August-3. September 2009, p. 165
MUSIL S., KRATZER J., VOBECKÝ M., MATOUŠEK T.: Chemical vapour generation of silver for AAS: A radiotracer study of generation, transport and trapping efficiency in quartz multiatomizer. In: CSI XXXVI – Colloquium Spectroscopicum Internationale, Book of Abstracts, Budapest, Hungary, 30. August-3. September 2009, p. 247
MATOUŠEK, T., MUSIL S., KRATZER J., ARSLAN, Y., HOVORKA J., BENADA O., VOBECKÝ M.: Generation of volatile species of transition and noble metals by aqueous tetrahydroborate. In: CSI XXXVI – Colloquium Spectroscopicum Internationale, Book of Abstracts, Budapest, Hungary, 30. August-3. September 2009, p. 108
MUSIL S., KRATZER J., VOBECKÝ M., MATOUSEK T.: Chemical Vapour Generation of Silver for Atomic Absorption Spectrometry: 111 Ag Radiotracer Study of Transport Efficiency and In-Situ Trapping on Quartz Surface. In: 5th Modern Analytical Chemistry, Prague, 21.-22.9 2009, p.51-57, ISBN: 978-80-86561-41-7
MUSIL S., KRATZER J., VOBECKÝ M., BENADA O., MATOUŠEK T.: Silver chemical vapor generation for atomic absorption spectrometry: method application, interference study and progress in analyte trapping on quartz surface. In: XIV. Czech-Slovak spectroscopic conference, Litomyšl, 31.5.-3.6.2010, p. Po-8, ISBN: 978-80-7395-282-2
SVOBODA M., TAURKOVÁ P., MUSIL S., MATOUŠEK T., RYCHLOVSKÝ P., DĚDINA J.: Investigation of Cryogenic Trapping for Arsenic Speciation Analysis by Hydride Generation – AAS and AFS. In: European Symposium on Atomic Spectrometry, Wroclaw, Poland, 5.-8.9. 2010, p. 114, ISBN: 978-83-927602-6-9
MUSIL S., KRATZER J., ARSLAN Y., VOBECKÝ M., BENADA O., MATOUŠEK T., RYCHLOVSKÝ P., ATAMAN O. Y., DĚDINA J.: Chemical Vapor Generation of Gold for AAS: 198,199Au Radiotracer Efficiency Study and Characterization of Gold Species. In: European Symposium on Atomic Spectrometry, Wroclaw, Poland, 5.-8.9. 2010, p. 115, ISBN: 978-83-927602-6-9
MUSIL S., ARSLAN Y., KRATZER J., VOBECKÝ M., BENADA O., MATOUŠEK T., RYCHLOVSKÝ P., ATAMAN O. Y., DĚDINA J.: Gold Chemical Vapor Generation by Tetrahydroborate Reduction for AAS: Radiotracer Efficiency Study and Characterization of Gold Species. In: 6th International Students Conference “Modern Analytical Chemistry”, Book of Proceedings, Prague, Czech Republic, 23.-24.9.2010, p. 11.-14., ISBN: 978-80-7444-005-2
SVOBODA M., MUSIL S., MATOUŠEK T., RYCHLOVSKÝ P., DĚDINA J.: Arsenic Speciation Analysis by Hydride Generation – Cryotrapping – Atomic Fluorescence Spectrometry with Flame-in-Gas-shield Atomizer. In: 6th International Students Conference “Modern Analytical Chemistry”, Book of Proceedings, Prague, Czech Republic, 23.-24.9.2010, p. 19.-22., ISBN: 978-80-7444-005-2
MUSIL S., MATOUŠEK T., SVOBODA M., SELECKÁ A., RYCHLOVSKÝ P., DĚDINA J.: Speciation analysis of arsenic by hydride generation-cryotrapping-atomic fluorescence spectrometry: achieving extremely low detection limits with inexpensive instrumentation. In: 3rd International Symposium on Metallomics, Münster, Germany, 15.-18.6.2011
DĚDINA J., MATOUŠEK T., KRATZER J., MUSIL S., SVOBODA M.: Generation of volatile species for trace and ultratrace elemental/speciation analysis with atomic absorption and atomic fluorescence detectors. In: Colloquium Spectroscopicum Internationale – CSI XXXVII, Book of Abstracts, Buzios, Rio de Janeiro, Brazil, 28.8.–2.9.2011, p. KL12, ISBN: 978-85-8006-046-1.
MUSIL S., KRATZER J., MATOUŠEK T., DĚDINA J.: Latest advances in volatile species generation of transition metals by tetrahydroborate reaction In: Colloquium Spectroscopicum Internationale – CSI XXXVII, Book of Abstracts, Buzios, Rio de Janeiro, Brazil, 28.8.–2.9.2011, p. OP37, ISBN: 978-85-8006-046-1.
MUSIL S., MATOUŠEK T., SVOBODA M., SELECKÁ A., RYCHLOVSKÝ P., DĚDINA J.: Speciation analysis of arsenic by hydride generation-cryotrapping-atomic fluorescence spectrometry: achieving extremely low detection limits with inexpensive instrumentation. In: Colloquium Spectroscopicum Internationale – CSI XXXVII, Book of Abstracts, Buzios, Rio de Janeiro, Brazil, 28.8.–2.9.2011, p. TH43, ISBN: 978-85-8006-046-1.
KRATZER J., MUSIL S., VOBECKÝ M., DĚDINA J.: Hydride trapping in quartz atomizers: possibilities and limitations. In: Book of abstracts 12th Rio Symposium on Atomic Spectrometry, 17.-21.9. 2012, Foz do Iguacu, Brazil, p. 64.
KRATZER J., MUSIL S., VOBECKÝ M., DĚDINA J.: In-atomizer trapping of hydrides for AAS – last advances. In: Book of abstracts European Symposium on Atomic Spectrometry 2012, XXth Slovak-Czech Spectroscopic Conference, 7.-12.10. 2012, Tatranská Lomnica, Slovakia, p. 72, ISBN 978-80-223-3292-7.
DĚDINA J., KRATZER J., MATOUŠEK T., MUSIL S., SVOBODA M.: Progress in trace elemental and speciation analysis based on volatile species generation and on atomic absorption/fluorescence detectors. In: Book of abstracts European Symposium on Atomic Spectrometry, XXth Slovak-Czech Spectroscopic Conference, 7.-12.10. 2012, Tatranská Lomnica,Slovakia, p. 27, ISBN 978-80-223-3292-7.
MATOUŠEK T., TROJÁNKOVÁ N., MUSIL S., CURRIER J. M., STÝBLO M., DĚDINA J.: Arsenic speciation analysis at (ultra)trace levels by hydride generation and/or HPLC with ICP MS detection – pros, cons and principal limitations of individual approaches. In: Book of abstracts European Symposium on Atomic Spectrometry, XXth Slovak-Czech Spectroscopic Conference, 7.-12.10. 2012, Tatranská Lomnica,Slovakia, p. 79, ISBN 978-80-223-3292-7.
DĚDINA J., KRATZER J., MATOUŠEK T., MUSIL S., SVOBODA M., CURRIER J.M., STÝBLO M.: Trace elemental and speciation analysis based on volatile species generation and on atomic absorption/fluorescence detectors – current state and perspectives. In: 12th International Symposium on Metal Ions in Biology and Medicine, 11.–13.3.2013, Punta del Este, Uruguay, p. 9, ISBN: 978-9974-0-0911-0.